WorksheetsMethods of Separation
Total questions: 20
Worksheet time: 10mins
A process in which centrifugal force is used to separate solid matter from a liquid suspension
Filtration
Centrifugation
Decantation
Distillation
Different types of Centrifuge
(Choose the possible correct answers)
Benchtop centrifuge
Swinging-bucket rotor
Fixed-head rotor
Vacuum Centrifuge
A process of pouring a liquid gently so as to not disturb a solid in the bottom of the container.
Centrifugation
Decantation
Filtration
Distillation
• A physical, biological or chemical operation that separates solid matter and fluid from a mixture with a filter medium that has a complex structure through which only the fluid can pass.
• Can be used instead of centrifugation for the separation of solids from liquids
Filtration
Decantation
Distillation
Centrifugation
The liquid that passes through the filter paper is called
Decantate
Sediment
Filtrate
Residue
Species other than the analyte that affect the final measurement are called
Interferents
Specimen
Filtrate
Result
A substances other than the analyte generate an instrumental readout similar to the analyte, such that the interference adds to the readout of the analyte
Difference
Result
Interference
Filtrate
A purification technique for a solid, usually organic. The separation is based on the solid’s solubility in a liquid solvent
Distillation
Liquid-Liquid Extraction
Solid-Liquid Extraction
Recrystallization
The key to the procedure is to use a maximum amount of solvent, such that the solid will just dissolve at the elevated temperature (usually the boiling point, if the solid is stable at that temperature).
True
False
A method of purification of liquids contaminated with either dissolved solids or miscible liquids
This method consist of boiling and evaporating the mixture recondensation of the vapors in a condenser
Distillation
Extraction
Filtration
Boiling
The separation is based on the fact that the contaminants have different boiling points than the liquid to be purified
The substances with lower boiling points are therefore separated from substances that have high boiling points
Filtration
Cooking
Distillation
Extraction
involves repeated evaporation–condensation steps before the distillate is actually collected
Simple Distillation
Extraction
Filtration
Fractional Distillation
Equipments that are used in simple distillation
(Choose all the possible correct answers)
Distilling flask
Condenser
Receiving Flask
Frationating Column
Thermometer
A method in which the analyte is removed from the original solvent and subsequently dissolved in a different solvent (extracted) while most of the remainder of the sample remains unextracted, i.e., remains behind in the original solution.
Solid-Liquid Extraction
Liquid-Liquid Extraction
Simple Distillation
Fractional Distillation
Criteria for successful separation of analyte:
Two liquids be immiscible and the analyte be more soluble in the extracting solvent than the original solvent
True
False
A laboratory apparatus that is manufactured especially for solvent extraction
Distilling Flask
Separatory funnel
Condenser
Beaker
Venting step is then repeated several times such that the two liquids have plenty of opportunity for the intimate contact required for the analyte to pass into the extracting solvent to the maximum possible extent
Shaking
Throwing
Filtrating
Distillating
This method is used when the analyte needs to be extracted from a solid material sample rather than a liquid
Liquid-Liquid Extraction
Solid-Liquid Extraction
Distillation
Filtration
During decantation, matter that settles to the bottom of a liquid
Sediment
Supernatant
Residue
Filtrate
Denoting the liquid lying above a solid residue after crystallization, precipitation, centrifugation, or other process.
Sediment
Residue
Supernatant
Filtrate
