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Organic Synthesis Quiz

Total questions: 24

Worksheet time: 13mins

Name
Class
Date
1.

What is the active oxidation state of the Pd catalyst in a Suzuki reaction?

a)

-2

b)

0

c)

+2

d)

+4

2.

Compound A - pKa 2

Compound B - pKa 4


Compound A is...

a)

2x more acidic than B

b)

10x more acidic than B

c)

100x more acidic than B

d)

2x more basic than B

3.

Which reagent would you use to reduce a carboxylic acid to an alcohol in presence of a ketone?

a)

LiAlH4

b)

BH3

c)

NaBH4

d)

Can't be done without protecting the ketone

4.

Which is the first elementary step of a Suzuki reaction catalysed by Pd(PPh3)4?

a)

Ligand exchange

b)

Oxidative addition

c)

Reductive elimination

d)

Transmetallation

5.

Which of these reactions contains a beta-hydride elimination step?

a)

Heck

b)

Sonogashira

c)

Suzuki

d)

All of the above

6.

What is the oxidation state change for the iodine atom in a Dess-Martin oxidation?

a)

I(V) to I(III)

b)

I(III) to I(V)

c)

I(III) to I(I)

d)

I(I) to I(III)

7.

Rank these N-heterocycles in order of basicity

a)

A > D > C > B

b)

A > B > C > D

c)

A > C > D > B

d)

A > C > B > D

8.

Which of these reactions does not generate a C-C bond?

a)

Stille

b)

Buchwald-Hartwig

c)

Sonogashira

d)

Negishi

9.

What is the name of this reaction?

a)

Negishi

b)

Stille

c)

Kumada

d)

Sonogashira

10.

Which of these is not required in a Swern oxidation?

a)

DMF

b)

DMSO

c)

Oxalyl chloride

d)

Triethylamine

11.

What is the name of this compound?

a)

Cholecalciferol (Vitamin D)

b)

Biotin (Vitamin B7)

c)

Pantothenic acid (Vitamin B5)

d)

Ascorbic acid (Vitamin C)

12.

Which is the most acidic proton in this molecule?

a)

A

b)

B

c)

C

d)

D

13.

Rank the following silyl protecting groups in order of stability in acid:

a)

TIPS > TBDPS > TBS > TES

b)

TBDPS > TBS > TIPS > TES

c)

TIPS > TBS > TBDPS > TES

d)

TBDPS > TIPS > TBS > TES

14.

What's the name of this molecule?

a)

1-Cl-6-Br-quinazoline

b)

1-Cl-6-Br-phthalazine

c)

4-Cl-7-Br-quinazoline

d)

4-Cl-7-Br-phthalazine

15.

Rank these heterocycles in order of SNAr reactivity

a)

C > B > D > A

b)

D > B > A > C

c)

B > A > C > D

d)

D > C > B > A

16.

Which of the following heterocycles can you not synthesise from hydrazine?

a)

Pyrazine

b)

Pyrazole

c)

Pyridazine

d)

Phthalazine

17.

Which of these is not a 1,3-dipole?

a)

Carbonyl ylide

b)

Sulfur ylide

c)

Diazomethane

d)

Ozone

18.

What is the name of this reaction?

a)

Fischer synthesis

b)

Vilsmeier reaction

c)

Hantzsch synthesis

d)

Mannich reaction

19.

What's the name of this molecule?

a)

5-chloro-2-methylthiazole

b)

5-chloro-2-methylisothiazole

c)

4-chloro-2-methylisothiazole

d)

4-chloro-2-methylthiazole

20.

Which of these structures corresponds to the TosMIC reagent?

a)

A

b)

B

c)

C

d)

D

21.

Which one of these alcohol protecting groups would be orthogonal to a N-Boc?

a)

O-PMB

b)

O-MOM

c)

O-THP

d)

O-TMS

22.

Which of these peptide coupling reagents doesn't require an additional base?

a)

HATU

b)

DCC

c)

CDI

d)

T3P

23.

Which pair of protecting groups will result in a shorter overall synthesis?

a)

A = THP, R = Bn

b)

A = Cbz, B = Me

c)

A = Boc, B = tBu

d)

A = Cbz, B = Bn

24.

Which product would you expect from this three step sequence?

a)

A

b)

B

c)

C

d)

D