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Acid–base titrations (Acidimetry and Alkalimetry)

Total questions: 20

Worksheet time: 10mins

Name
Class
Date
1.

Describe in detail acid–base titrations by selecting all statements that correctly summarize their key features, reagents, and defining reaction.

a)

They involve a neutralization process between an acid and a base forming salt and water.

b)

The characteristic reaction for these titrations is H++OHH2OH^+ + OH^- \rightarrow H_2O .

c)

In this context, an acid is defined as a substance that, when dissolved in water, gives OHOH^- ions.

d)

A base is a substance that, when dissolved in water, gives OHOH^- ions.

e)

Commonly used reagents include acids such as HCl and H2SO4H_2SO_4 and bases such as NaOH, KOH, and sodium bicarbonate.

2.

In the assay of sodium bicarbonate, which titration method is used?

a)

Acidimetric method

b)

Alkalimetric method

c)

Argentimetric method

d)

Complexometric method

3.

What is the chemical formula of sodium bicarbonate used in the direct titration method of its assay?

a)

NaHCO3

b)

Na2CO3

c)

Na2HPO4

d)

NaCl

4.

Which statements form the stated principle of the sodium bicarbonate assay?

a)

Sodium bicarbonate is titrated by an acidimetric method

b)

Sodium bicarbonate, a salt of strong base NaOH and carbonic acid, is dissolved in water

c)

The alkaline solution is directly titrated with strong acids like HCl using methyl orange

d)

The assay requires argentometric precipitation with silver nitrate

5.

For preparing 1 M hydrochloric acid for the assay, what volume of commercial concentrated HCl is diluted to make 100 ml?

a)

8.9 ml

b)

1.5 ml

c)

0.1 ml

d)

27.0 ml

6.

In preparing 1 M HCl, to what final volume is the solution made up with distilled water?

a)

100 ml

b)

250 ml

c)

500 ml

d)

50 ml

7.

At approximately what temperature is anhydrous sodium carbonate previously heated for 1 hour before use in standardization?

a)

270C270^\circ\text{C}

b)

100C100^\circ\text{C}

c)

150C150^\circ\text{C}

d)

350C350^\circ\text{C}

8.

For standardizing HCl in this procedure, what volume of water is used to dissolve the weighed sodium carbonate in a 250 ml conical flask?

a)

100 ml

b)

50 ml

c)

150 ml

d)

200 ml

9.

Which indicator and amount are added during the standardization of hydrochloric acid in this assay?

a)

0.1 ml of methyl red solution

b)

3 drops of phenolphthalein solution

c)

0.5 ml of methyl orange solution

d)

1.0 ml of bromothymol blue solution

10.

Assay of boric acid/boracic acid is performed by which titrimetric method?

a)

Acid–base alkalimetric direct titration of boric acid dissolved in a glycerin–water mixture using phenolphthalein and standardized NaOH

b)

Redox titration with potassium permanganate in acidic medium using a self-indicator

c)

Non-aqueous titration with perchloric acid in glacial acetic acid using crystal violet

d)

Argentometric titration of borate with silver nitrate using potassium chromate

11.

According to the described assay of ammoniated mercury, which type of titration is used?

a)

Acid–base titration (indirect titration)

b)

Redox titration

c)

Complexometric titration

d)

Non-aqueous titration

12.

In the worksheet section on the assay of ammoniated mercury, what is the chemical formula stated for ammoniated mercury?

a)

NH2HgCl

b)

NH4HgCl

c)

HgNH2Cl2

d)

NH2HgBr

13.

In the principle of the assay, the sample is dissolved in a solution of which reagent before further treatment?

a)

Potassium iodide

b)

Sodium chloride

c)

Potassium bromide

d)

Ammonium nitrate

14.

During the assay, the precipitate of HgCl2 dissolves in excess potassium iodide with liberation of equivalent alkalies. Which alkalies are titrated against standard acid using methyl orange as indicator?

a)

Ammonia and KOH

b)

NaOH and NH4OH

c)

K2CO3 and NH3

d)

Ca(OH)2 and NH3

15.

Which titrant and indicator are specified for titrating the liberated alkali in the assay of ammoniated mercury?

a)

0.1 N HCl using methyl orange

b)

0.1 N NaOH using phenolphthalein

c)

0.05 N H2SO4 using methyl red

d)

0.1 N HCl using phenolphthalein

16.

According to the listed reactions, what soluble product forms when HgCl2 reacts with 2 KI during the assay?

a)

K2HgI4

b)

HgI2

c)

K2HgCl4

d)

KI3

17.

Which category is assigned to ammoniated mercury in the worksheet?

a)

Topical antiseptic and disinfectant

b)

Systemic antibiotic

c)

Analgesic and antipyretic

d)

Topical corticosteroid

18.

Which listed use is given for ammoniated mercury in the worksheet?

a)

In treatment of psoriasis

b)

Management of hypertension

c)

Oral contraceptive

d)

Treatment of diabetes mellitus

19.

Which additional use is stated for ammoniated mercury?

a)

To treat minor skin infections and other skin disorders

b)

To relieve migraine headaches

c)

To treat asthma exacerbations

d)

To manage cardiac arrhythmias

20.

Assay of Ammonium Chloride (I.P. 1985): Select all statements that correctly describe the method and standard as presented in the note on the assay of ammonium chloride.

a)

It is an acid–base titration performed by an indirect titration method.

b)

A weighed quantity of ammonium chloride is dissolved in water and treated with neutralised formaldehyde.

c)

The liberated HCl is titrated with standard sodium hydroxide using phenolphthalein to a pink end point.

d)

The assay uses 0.1 N sulfuric acid with methyl orange as the indicator.

e)

The I.P. standard requires not less than 99% and not more than 100.5% of NH4Cl.